The vendor inspects, cleans, and calibrates balances on site. Calibrate the analytical balance or the microbalance. h. Note that the acceptable tolerance varies for the 10 and 100 mg reference weights, depending upon whether they are being weighed on a top loading balance that reads to 0.01g or a more sensitive analytical balance. METTLER TOLEDO's Excellence Level analytical balances have built-in functionalities to ensure that weighing is always in the safe weighing range of the balance. 8.3 CALIBRATION 8.3.1 At least once a year, when balances are moved off of a physical surface, or as deemed necessary, the current user shall check all analytical and electronic balances with standard weights. 0000011054 00000 n RESPONSIBILITY Officer/ Executive – Quality Control ACCOUNTABILITY Head QC/QA PROCEDURE Description of balance: XS 204 DR is analytical class balance with a touch screen display terminal … After calibration, the balance will enter weighing mode 4. head - quality control – to ensure the compliance of the sop. The opinions and conclusions stated are those of the author and may or may not be those of the Laboratory. National Library of Australia Cataloguing-in-Publication En!ry Prowse, David B., 1938-The calibration of balances. 5.5 After few seconds, the display will show 0.00 g. 5.6 If display is not stable, press the TARE key & wait till the display shows 0.00 g. 5.7 Perform internal calibration and in Annexure-II 5.6 For Accuracy 5.6.1 Place 5 gm. 0000182206 00000 n BWhen weighed on a top loading balance that reads to 0.01g. 0000010176 00000 n 0000007077 00000 n Definition of Validation: USP: “Validation of an analytical procedure is the process by which it is established, by laboratory studies, that the performance characteristics of the procedure meet the requirements for the intended analytical applications.” 4. CarePac® weight sets contain only two weights – which is all that is required for routine balance testing between calibrations. 3.0 responsibility: microbiologist – to perform the operation as per sop. 0000006616 00000 n 0000202338 00000 n 0000238009 00000 n VERIFYING CALIBRATION OF WEIGHING DEVICES USED FOR LABORATORY TESTING TXDOT DESIGNATION: TEX-901-K … Analytical instruments are used for a specific analysis. 2. Standard Operating Procedure (SOP) for operation and calibration of analytical balances. %PDF-1.2 %���� 0000010784 00000 n 6. Drift check. But the thumb rule followed in pharmaceutical industries for lower limit is least count X 50 and upper limit is 80% of capacity of the balance. 5.8.2 When the balance stabilizes take the print out. 0000021279 00000 n Introduction In most facilities, the balance is a critical item of equipment which must operate correctly and have suitable traceability in order to ensure the quality of test results. 0000018513 00000 n 0000015065 00000 n 0000151712 00000 n Note: After calibration, check that the tolerance between the displayed value and the calibration weight value is no more than ±0.0002 g. g. See section 12.4 for acceptable tolerances for weigh balances when conducting the accuracy check. Calibration.....5 b. Verification ... analytical balance.....32 Table 5: Primary data obtained from the drift assay on 17/09/09 for an analytical balance. It applies to both gas-operated and liquid-operated pressure balances. 0000008422 00000 n 0000040697 00000 n LAB-101. 0000003295 00000 n INTRODUCTION: The ability to determine mass accurately is fundamental not only to analytical chemistry but also to all of modern science. Analytical balances are accurate and actual equipment used to evaluate public. 8.2.2 Procedure for Mettler XS205 (#2) 1. 0000008275 00000 n 0000006491 00000 n 0000040672 00000 n 0000004815 00000 n Unload the weight and repeat the procedure for all the weights. In both cases the method is a comparative one. Uncertainty in measurement & Pan Corner Test: Place 100 mg standard weight in four corners and middle of the balance and note down the readings . The above procedure (Referred under Section 5.1.1. to 5.1.4.) To turn the balance off, press the OFF key on the panel and the dis- calibration weight used in sensitivity adjustment. If the balance cannot be shut down in an emergency situations, people can be injured or the balance Analytical Balance Calibration Learn how to calibrate the Analytical Balance as Drift check, Performance check and Measurement uncertainty check. Constant temperature is … {­èôZÑèÄuŸèÄÅ)ÅùåsöûHpž[°8sG­”!X ™Î¢÷ýiC.5ÿlßZÕ¥ûõ­. The equipment verification was performed on balances and analytical balances, liquid chromatographs and gas chromatographs. 0000016984 00000 n 0000006785 00000 n Internal Calibration: Internal calibration doesn’t require manual efforts. on the weighing pan. All equipments used in the production of products shall be properly Validated and Calibrated “to demonstrate that it is suitable for its intended purpose”. Topics include calibration procedures, operation of mechanical and electronic balances, use of weighing vessels for solids, use of gas tight syringes for liquids, and best practices for solution preparation. 1292 0 obj << /Linearized 1 /O 1294 /H [ 3295 404 ] /L 863885 /E 238541 /N 10 /T 837925 >> endobj xref 1292 144 0000000016 00000 n Balance drift can be present without the operators being aware of the problem. CALIBRATION OF TOP PAN BALANCE Calibration procedure: Internal calibration It shall be performed as per the manufacturer’s instructions. 0000008717 00000 n 0000020806 00000 n 0000009179 00000 n 0000022326 00000 n For best results, ... 2. Maintenance and Calibration of Analytical Balance Document No. 0000025459 00000 n So regular performance verifications are made to ensure that the instrument to be used is suitable for its intended application. b. laoconco 3 LL L Specifications Model LAB-101 LAB-102 LAB-103 LAB-104 Capacity 0-100 g 0-200 g 0-300 g 0-400 g Readability 1 … 1.1 This guideline describes calibration methods for pressure balances including an example of an uncertainty estimation for the use of a pressure balance. Acceptance Criteria: % RSD: NMT 0.1 % for pan corner … 0000007832 00000 n 0000006763 00000 n 0000018537 00000 n How to Calibrate an Analytical Balance? Weigh Balance Calibration Record Form (section 14). 0000009614 00000 n 0000009302 00000 n Record the observations in balance calibration record format. 0000005931 00000 n 0000003676 00000 n 3. Unpacking the Balance Unpack the balance carefully. 0000202313 00000 n Practically speaking, all measurements which we shall perform in this course relate either directly or indirectly to a weighing using the single pan analytical balance. These days, Essae-Teraoka analytical balances provide a superior mixture of perfection, precision and value. It includes calibration of analytical instruments like UV, IR, and HPLC. Technique for the calibration of a Mettler Analytical balance. 0000016267 00000 n Work room should be clean and dry 2. VERIFYING CALIBRATION OF WEIGHING DEVICES USED FOR LABORATORY TESTING TXDOT DESIGNATION: TEX-901-K CONSTRUCTION DIVISION 2 – 5 EFFECTIVE DATE: AUGUST 1999 3.2.3 Table 1 lists weight classes used for calibration, either as external or internal balance weights mechanically selected by the operator. 2. using an analytical balance. Chart 1. 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